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N-methyl-Methylcyclohexylamine CAS 100-60-7
2022-02-21 11:09  Click:70
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Descriptions

Synonyms

Cyclohexylmethylaminecyclohexyl-methyl-aminemethylcyclohexylamine,[corrosivelabel]Cyclohexylamine,N-methyl-1-MethylcyclohexylamineCyclohexanamine,N-methyl-MethylcyclohexylamineN-Cyclohexylmethylamine

CAS No.100-60-7

Molecular FormulaC7H15N ( Isomeride)

Molecular Weight113.204

EINECS202-869-3

CategoryPharmaceutical Intermediates

N-methyl-Methylcyclohexylamine CAS 100-60-7


Physicochemical properties

Density0.868

Melting point-8℃

Boiling point149℃

Refractive index1.4545-1.4565

Flash point29℃

Vapor pressure4.62mmHg at 25°C

PSA12.03000

logP1.92940

Appearancetransparent and colorless liquid

Color colorless liquid

Physical Propertytransparent and colorless liquidMiscible with various organic solvents, slightly soluble in waterMelting point:&#87229-&#87227 &#x00b0C(lit.) Boiling point149 &#x00b0C(lit.) Density0.868&#160g/mL&#160at 25 &#x00b0C(lit.) Refractive indexn20/D 1.456(lit.) Flash point85 &#x00b0F Water solubility5.4 g/100 mL (20 &#186C) transparent and colorless liquid. Miscible with various organic solvents, slightly soluble in watertransparent and colorless liquidBoiling point 147~151℃ Relative density 0.868 Refractive index 1.4456 Flash point 29℃ Solubility  Miscible with various organic solvents, slightly soluble in water

SolubilitySlightly soluble in water, soluble in benzene, alcohol, etc


Application

Used as intermediates in medicine and dyes

Pharmaceutical and dye intermediates. Used as an intermediate in the drug bromohexamine hydrochloride


Production Method

With cyclohexylamine as raw material prepared. 2. By the reaction of cyclohexanone and methylamine. Soak aluminum sheet in methanol, add high mercury chloride, continue to soak 2h, temperature rise does not exceed 55℃, remove the soaking liquid. Add ethanol to the activated aluminum sheet, drop the mixture of methylamine and cyclohexanone under agitation, heat reflux, and place overnight. Adding 10% sodium hydroxide solution alkalization, extracting with benzene twice, after washing by distillation, benzene recovery that distillation of n-methyl cyclohexylamine. The yield is about 80%. ;


Storage and transport information

It should be sealed and stored in a dry and cool ventilated warehouse


Packaging

200KG/ drum storage: It is recommended to store in dry and cool areas and properly ventilated. After the original packaging, please fasten the packaging cover as soon as possible to prevent moisture and other substances from mixing and affecting the product performance. Do not inhale dust and avoid skin and mucous membrane contact. Smoking, eating and drinking are prohibited in the workplace. After work, shower and change. Store contaminated clothes separately and reuse them after washing. Maintain good hygiene.




Contact Us

SHANGHAI OHANS CO., LTD.

Factory Address Jining High-tech Development Zone, Shandong, China

Call Center 021-5161-9971

Headquarters Room a2110, building 55, No. 709, Lingshi Road, Zhabei District, Shanghai

Email Us honda@ohans.com  candy@ohans.com

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